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Beilstein J. Org. Chem. 2013, 9, 1713–1717, doi:10.3762/bjoc.9.196
Graphical Abstract
Scheme 1: The effect of water in radical multifunctionalization reactions.
Scheme 2: Transformation of 3 into 5-amino-1,4-diol derivative 25.
Scheme 3: Proposed reaction mechanism.
Beilstein J. Org. Chem. 2013, 9, 675–680, doi:10.3762/bjoc.9.76
Scheme 1: Aldehydes and ketones are reduced by 1 when silica gel is added.
Scheme 2: Pilot reduction of aldehyde 2 with 1 and acetic acid.
Figure 1: 11B NMR studies of boron products from 1 and acetic acid with and without aldehyde 2. aIn C6D6; bun...
Scheme 3: Chemoselective reductions of aldehydes with 1 and acetic acid. aDetermined by 1H NMR spectroscopic ...